Oxidized diffusion barrier surface for the adherence of copper a

Semiconductor device manufacturing: process – Coating with electrically or thermally conductive material – To form ohmic contact to semiconductive material

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438648, 438653, 438658, 438677, 438687, H01L 213065, H01L 21310

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active

059131446

ABSTRACT:
A method has been provided for improving the adhesion of Cu to a diffusion barrier material, such as TiN, in an integrated circuit substrate. The diffusion barrier is exposed to either a reactive oxygen species, or a plasma containing oxygen. A thin layer of the diffusion barrier is oxidized, typically less than 50 .ANG., in response to exposure to the oxygen environment. CVD copper is then deposited over the oxidized diffusion barrier surface. The oxide layer improves bonding between the copper and diffusion barrier surfaces. The oxide layer permits the control of tolerances in the diffusion barrier preparation processes, and copper precursor, to be relaxed. An integrated circuit comprising an oxide layer between the diffusion barrier and the copper layer is also provided.

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Article entitled "Copper Interconnection with Tungsten Cladding for ULSI" presented at the 1991 Symposium on VLSI Technology, Digest of Technical Papers, May 28-30, 1991, pp. 37-40. (Cho et al.).
Article entitled Encapsulated Copper Interconnection Devices Using Sidewall Barriers, presented at the 1991 VMIC Conference, Jun. 11-12, 1991, pp. 99-108. (Gardner et al.).

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