Method for purifying 3',5'-cyclic-adenylic acid or 3',5'-cyclic-

Details Method for purifying 3',5'-cyclic-adenylic acid or 3',5'-cyclic- Method for purifying 3',5'-cyclic-adenylic acid or 3',5'-cyclic-

1973-12-06

1976-03-02

Brown, Johnnie R.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07H 1920

Patent

active

039417700

ABSTRACT:
3' ,5'-Cyclic-adenylic acid or 3' ,5'-cyclic-deoxadenylic acid can be obtained in a high purity and a high yield by adding a water-soluble organic solvent such as methyl alcohol, ethyl alcohol, n-propyl alcohol, isopropyl alcohol, tert-butyl alcohol, acetone, N,N'-dimethylformamide, dioxane, tetrahydrafuran, ethyleneglycolmonomethylether and the like singly or in combination to an aqueous solution containing as impurities one or more kinds of nucleotides other than 3' ,5'-cyclicadenylic acid and 3' ,5'-cyclic-deoxyadenylic acid, nucleosides, nucleobases, colored substances, proteins and the like in addition to 3' ,5'-cyclic-adenylic acid or 3', 5'-cyclic-deoxyadenylic acid.
The said 3' ,5'-cyclic-adenylic acid or 3' ,5'-cyclic-deoxyadenylic acid are useful and valuable as a biochemical reagent.

REFERENCES:
patent: 3157636 (1964-11-01), Sanno et al.
patent: 3190877 (1965-06-01), Ishibashi et al.
patent: 3215687 (1965-11-01), Tsuchiya et al.
patent: 3287232 (1966-11-01), Mitsugi et al.
patent: 3457254 (1969-07-01), Yano et al.

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