Method and apparatus for implement XANES analysis

X-ray or gamma ray systems or devices – Specific application – Absorption

Reexamination Certificate

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C378S053000, C378S084000

Reexamination Certificate

active

11291349

ABSTRACT:
Compact, low-power-consuming systems and methods for exposing samples to high-energy radiation, for example, for exposing samples to x-rays for implementing x-ray absorption near edge analysis (XANES). The systems and methods include a low-power-consuming radiation source, such as an x-ray tube; one or more tunable crystal optics for directing and varying the energy of the radiation onto a sample under analysis; and a radiation detecting device, such as an x-ray detector, for detecting radiation emitted by the sample. The one or more tunable crystal optics may be doubly-curved crystal optics. The components of the system may be arranged in a collinear fashion. The disclosed systems and methods are particularly applicable to XANES analysis, for example, XANES analysis of the chemical state of chromium or another transition metal in biological processes.

REFERENCES:
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patent: 2002/0131550 (2002-09-01), Fujioka et al.
patent: 06 313757 (1994-11-01), None
patent: 2001 021507 (2001-01-01), None
Z. Chen et al., “Microanalysis by Monochromatic Microprobe X-Ray Fluorescence-Physical Basis, Properties, and Future Prospects”, Journal of Applied Physics, American Institute of Physics, vol. 84, No. 2, pp. 1064-1073 (Jul. 15, 1998).
Z. Chen et al., “Microprobe X-Ray Fluorescence With the Use of Point-Focusing Diffractors”, Applied Physics Letters, American Institute of Physics, vol. 71, No. 13, pp. 1884-1886 (Sep. 29, 1997).

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