Method and apparatus for oxygen delignification

Paper making and fiber liberation – Processes of chemical liberation – recovery or purification... – Continuous chemical treatment or continuous charging or...

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162 37, 162 38, 162 57, 162 65, 162239, 162241, 162243, 422190, 422234, D21C 700, D21C 910, D21C 1106

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043849202

ABSTRACT:
An apparatus and process for the oxygen delignification of pulp is provided in which the pulp is transported by means of timing screws in essentially plug flow through one or more substantially horizontal reactor tubes. Oxygen gas is injected into the system at a point adjacent to the pulp inlet and travels concurrently in substantially plug flow with the pulp through the system. In this manner, the pulp is initially exposed to gas of a high oxygen partial pressure while gas vented from the system adjacent the pulp outlet is of low oxygen partial pressure and has a high content of diluent gases. The process and apparatus avoid the formation of gas pockets and hot spots which may adversely affect the pulp. In an alternate embodiment, a countercurrent gas flow process is disclosed. Also provided is a catalytic treatment and recirculation system for the vented gas which permits efficient use of oxygen within the system.

REFERENCES:
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patent: 3832276 (1974-08-01), Roymoulik
patent: 3964962 (1976-06-01), Carlsmith
patent: 4050981 (1977-09-01), Jamieson et al.
patent: 4093511 (1978-06-01), Richter
patent: 4161421 (1979-07-01), Sherman
patent: 4177105 (1979-12-01), Laakso et al.
patent: 4248662 (1981-02-01), Wallick
Chang et al., "Delignification of High Yield Pulps with Oxygen and Alkali", TAPPI, vol. 57, No. 5, May 1974, p. 123.
Annergren et al., "An Alternative to High Consistency Oxygen Bleaching", 1979, Pulp Bleaching Conf., Toronto, Canada, Jun. 11-14, 1979, p. 99.
Nusmar et al., "Medium Consistency Oxygen Bleaching", TAPPI, vol. 63, No. 4, Apr. 1980, p. 105.
Myburgh, "Operations of the Enstra Oxygen Bleaching Plant", TAPPI, vol. 57, No. 5, May 1974, p. 131.
Hillstrom et al., "Process Concepts for Oxygen Delignification", Svensk Paperstid, vol. 80, pp. 167-170, Apr. 1977.
Luthi et al., "Gas Concentration and Temperature Distribution in Oxygen Delignification", presented at the TAPPI Alkaline Pulping Conference, Washington, D.C., Nov. 7-10, 1977.
Evans et al., "The Kinetics of Low Consistency Oxygen Delignification", TAPPI, vol. 62, No. 6, Jun. 1979, pp. 37-39.

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