Whey protein products

Food or edible material: processes – compositions – and products – Products per se – or processes of preparing or treating... – Protein – amino acid – or yeast containing

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C426S583000

Reexamination Certificate

active

06383551

ABSTRACT:

FIELD OF THE INVENTION
The present invention relates to methods of forming whey protein products having desirable physical properties, and the whey protein products so formed.
BACKGROUND OF THE INVENTION
Milk whey protein is prepared by removing fat and casein from milk, and comprises &agr;-lactalbumin, &bgr;-lactoglobulin and whey albumin. The main whey protein is &bgr;-lactoglobulin (&bgr;-lg), which constitutes about 50% of the total whey proteins. Large amounts of whey proteins are produced during the manufacturing of dairy products. The nutritional value of whey proteins makes them useful as food ingredients.
Whey proteins can be used as a protein source in desserts; however, it has been difficult to produce whey protein desserts with an acceptable texture without adding carbohydrate gelling agents (Mleko,
Milchwissenshaft
52:262-265, 1997). The viscosity of whey protein dispersions is related to the size and shape of the protein molecules. Food proteins, especially whey proteins, are small (<60 kDa) and more spherical in shape compared to carbohydrate hydrocolloids which are large (generally>200 kDa) and rod-like. For coiled molecules, the viscosity is a function of the diameter of the coil and of the extent to which solvent can drain freely through the coil without becoming entrapped by hydrodynamic forces. For a homologous series of rods of constant diameter, the viscosity increases with molecular weight, which is proportional to the length (Cantor and Schimmel 1980,
Biophysical Chemistry. Part II: Techniques for the study of biological structure and function,
W. H. Freeman and Company, San Francisco, Calif.).
The functionality of a protein or polysaccharide is associated with specific chemical and physical properties of individual macromolecules, interactions with other ingredients, and the processing operations used in producing a given food. Food proteins and carbohydrate hydrocolloids differ in functionality. For example, the viscosity of carbohydrate hydrocolloids can be several hundred times higher than food proteins at the same concentration. To be acceptable for use in food products, whey protein products must have acceptable physical properties and acceptable mouth feel.
Accordingly, it is desirable to obtain whey protein dispersions with viscosities comparable to that of carbohydrate hydrocolloids.
SUMMARY OF THE INVENTION
In view of the foregoing, a first aspect of the present invention is a method of producing a whey protein product using a solution of at least about 2% whey proteins with a pH of at least about 8.0, which is heated and then cooled. The pH of the whey protein solution is adjusted to less than about pH 8.0, and the whey protein solution is heated in a second heating step to produce a whey protein product.
A second aspect of the present invention is a method of producing a whey protein product using a first solution of whey proteins having a pH of at least about 8.0, heating and then cooling this first solution, and then diluting the solution to provide a diluted whey protein solution. The pH of the diluted whey protein solution is adjusted to less than about 8.0, and it is heated in a second heating step to produce a whey protein product.
A further aspect of the present invention is a method of producing a whey protein product by providing a first solution of whey proteins having a concentration of about 4%. whey proteins and a pH of about 8.0, heating this solution in a first heating step at a temperature of at least about 75° C. and then cooling to a temperature below the gellation point of the whey proteins. The resulting whey protein solution is diluted to a concentration of from about 2.5% to about 3.5% whey proteins and the pH is adjusted to about 7.0. The diluted whey protein solution is heated in a second heating step at a temperature of at least about 75° C. to produce a whey protein product.
A further aspect of the present invention is a method of producing a whey protein product using a whey protein solution having a concentration of about 4% whey proteins and a pH of about 8.0, which is heated in a first heating step at a temperature of at least about 75° C. and then cooled to a temperature below the gellation point of the whey proteins. The pH of the solution is adjusted to about 7.0, and it is heated in a second heating step at a temperature of at least about 75° C. to produce a whey protein product.
A further aspect of the present invention is a whey protein dispersion having a viscosity of from about 200 to about 550 mPa s when measured at 50 l/s, having a concentration of whey proteins from about 2.0% to about 5.0%, and having an optical density of less than about 1.5 when measured at 630 nm.


REFERENCES:
patent: 4675201 (1987-06-01), Lee et al.
patent: 4734287 (1988-03-01), Singer et al.
patent: 5217741 (1993-06-01), Kawachi et al.
patent: 5232729 (1993-08-01), Katsuta et al.
patent: 5350590 (1994-09-01), McCarthy et al.
patent: 5416196 (1995-05-01), Kitabatake et al.
patent: 5503864 (1996-04-01), Uchida et al.
Bagley and Christianson et al.; Swelling Capacity Of Starch And Its Relationship To Suspension Viscocity-Effect Of Cooking Time, Temperature and Concentration,Journal of Texture Studies, 13:115-126 (1982).
Barnes; Shear—Thickening (“Dilatancy”) in Suspensions of Nonaggregating Solid Particles Dispersed in Newtonian Liquids,Journal of Rheology, 33(2):329-366 (1989).
Boersma et al.; Computer simulations of shear thickening of concentrated dispersions,Journal of Rheology, 39(5):841-860 (1995).
Chow et al.; Gap size and shear history dependencies in shear thickening of a suspension ordered at rest,Journal of Rheology, 39(1):15-32 (1995).
Daubert and Foegeding, Rheological Principles for Food Analysis,Introduction to Food Analysis, Chapter 34, (Nielsen, Ed.) Chapman & Hall, N.Y. pp. 553-569 (1998).
Dintzis et al.; Shear-thickening and flow-induced structure in a system of DMSO containing waxy maize starch,Journal of Rheology, 39(6):1399-1408 (1995).
Goerges et al.; Etude thermodynamique de la dissociation réversible de la &bgr;-lactoglobuline B pour des pH supérieurs á 5,5,Biochim Biophys. Acta., 59:737-739 (1962).
Hoch; Whey to Go,Food Processing, 3:51-52 (1997).
Hoffmann;&bgr;-Lactoglobuline: denaturation and aggregation, PH.D Thesis, Universiteit Utrecht (1997).
Hoffmann et al.; Aggregation of &bgr;-lactoglobulin studied by in situ light scattering,Journal of Dairy Research, 63:423-440 (1996).
Hoffmann, et al.; Molecular Mass Distrubutions of Heat-Induced &bgr;-Lactoglobulin Aggregates,J. Agric. Food Chem., 45:2949-2957 (1997).
Huffman, Processing Whey Protein for Use as a Food Ingredient,Food Technology, 2:49-52 (1996).
Iametti et al.; Modifications occur at different structural levels during the heat denauration of &bgr;-lactoglobulin,Eur. J. Biochem., 237:106-112 (1996).
Langton and Hermansson; Fine-stranded and particulate gels of &bgr;-lactoglobulin and whey protein at varying pH,Food Hydrocolloids, 5(6):523-539 (1992).
McKenzie and Sawyer; Effect of pH on &bgr;-Lactoglobulins,Nature, 214:110101104 (1967).
Mleko; Effect of pH on the Microstructure and Texture of Whey Protein Concentrates and Isolate Gels,Polish Journal of Food and Nutrition Sciences, 5/46(1):63-72 (1996).
Mleko; Rheological properties of milk and why protein desserts,Milchwissenschaft, 52(5):262-265 (1997).
Qi et al.; Effect of temperature on the secondary structure of &bgr;-lactoglobulin at pH6.7, as determined by CD and IR spectroscopy: a test of the motion globule hypothesis,Biochem J., 324:3410346 (1997).
Shimada and Cheftel; Sulfhydryl Group/Disulfide Bond Interchange Reactions during Heat-Induced Gelation of Whey Protein Isolate,J. Agric. Food Chem., 37:161-168 (1989).
Silva et al.; Granule Size Distribution and Rheological Behavior of Heated Modified Waxy and Unmodified Maize Starch Dispersions,Journal of Texture Studies, 28: 128-138 (1997).
Watanabe and Klostermeyer; Heat-induced changes in sulphydryl and disulphide levels of &bgr;-lactoglobulin A and the formation of polymers,J. Dairy Research, 43:411-418 (1976).

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Whey protein products does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Whey protein products, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Whey protein products will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-2902888

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.