Vertical spray etch reactor and method

Adhesive bonding and miscellaneous chemical manufacture – Delaminating processes adapted for specified product – Delaminating in preparation for post processing recycling step

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156345, 156642, 156656, 1566591, 156666, 156902, C23F 102, B44C 122, C03C 1500, C03C 2506

Patent

active

049043390

ABSTRACT:
Vertical spray etch reactor and method in which a nitric acid etching solution is sprayed onto an upright workpiece in the form of low impact, large drops to produce a gentle sheeting flow of the etching solution down the workpiece. The solution is sprayed in a generally trapezoidal pattern with the greater portion of solution being sprayed onto the upper portion of the workpiece. The etching solution is delivered to the spray nozzles by a low shear positive displacement pump. As the workpiece leaves the etch chamber, it is sprayed with a solution to remove the etching solution and dissolved copper and to adsorb gaseous by-products from the etching reaction. The rinsing solution is collected and utilized to replenish the etching solution. The workpiece receives additional rinsing in a third chamber, and gases are exhausted from the system through an exhaust vent in the third chamber. Air is introduced into the etch chamber to move the gaseous by-products toward the exhaust vent.

REFERENCES:
patent: 4017343 (1977-04-01), Haas
patent: 4371422 (1983-02-01), Eidschun
patent: 4376009 (1983-03-01), Kunz
patent: 4454003 (1984-06-01), Fishman et al.
patent: 4482425 (1984-11-01), Battey
patent: 4497687 (1985-02-01), Nelson
patent: 4545850 (1985-10-01), Nelson
patent: 4620894 (1986-11-01), Gurian et al.

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