Electric resistance heating devices – Heating devices – Continuous flow type fluid heater
Reexamination Certificate
2001-01-09
2002-12-24
Walberg, Teresa (Department: 3742)
Electric resistance heating devices
Heating devices
Continuous flow type fluid heater
C392S496000, C134S107000
Reexamination Certificate
active
06498898
ABSTRACT:
FIELD OF THE INVENTION
The present invention generally relates to methods and apparatuses for delivery of fluids in a processing system used for the fabrication of integrated circuits and flat panel displays. Specifically, the present invention relates to methods and apparatuses for heating fluid delivery lines in a vacuum processing system in order to heat the fluid flowing therein and for containing fluid leaked from the fluid delivery lines.
BACKGROUND OF THE INVENTION
Vacuum processing systems for processing 100 mm, 200 mm, 300 mm or other diameter wafers are generally known. Typically, such vacuum processing systems have a centralized transfer chamber mounted on a monolith platform. The transfer chamber is the center of activity for the movement of substrates being processed in the system. One or more process chambers and load lock chambers mount on the transfer chamber, and a transfer chamber robot mounts in the middle of the transfer chamber to access each of the process chambers and load lock chambers to transfer a substrate therebetween. Different process chambers perform different processes on the substrates. For example, a physical vapor deposition (PVD) chamber or a chemical vapor deposition (CVD) chamber may deposit a layer of material, such as a conductor or an insulator, onto the surface of the substrate; or an etch chamber may remove a layer of material from parts of the surface of the substrate; or an ion implantation chamber may implant ion dopants into the substrate; or a pre-clean chamber may remove a layer of the substrate contaminated with oxides; or a thermal processing chamber may heat a substrate to cure or anneal the substrate after a previous process. In fact, it is not uncommon for a manufacturer of semiconductor processing systems to provide over twenty different types of process chambers. Access to the transfer chamber from the clean ambient environment is typically through the load lock chambers. The load lock chambers may open to a very clean room, referred to as the white area, or to a substrate handling chamber, typically referred to as a mini-environment, for transferring substrates in a very clean environment at atmospheric pressure from pods seated on pod loaders to the load lock chambers.
Each type of process chamber typically performs one specific step or series of steps in the overall fabrication of integrated circuits or flat panel displays. For example, some types of process chambers specifically deposit one particular material onto the surface of the wafer. Other types of process chambers specifically etch away a particular layer from the surface of the wafer. Still other types of process chambers specifically implant a particular ion into the wafer.
Many of these processes require that certain gases or liquids be delivered to the process chamber to perform the process. These gases and liquids are commonly called process fluids and are delivered to the process chambers through fluid delivery lines from sources of the fluids in the manufacturing plant. For example, a chemical vapor deposition process of copper may require cupraselect, a metal organic compound, be provided as a precursor in the process. Another process may use dimethylaluminumhydride (DMAH) to perform chemical vapor deposition of aluminum. Yet another process may use tetrakisdimethylaminotitanium (TDMAT) to deposit a film of titanium nitride on a wafer. Still another process may use barium and strontium precursors to deposit a film of barium strontium titanate (BST). The process fluids are typically converted into a gaseous state by vaporization, bubbling or other appropriate process to deliver a vapor of the process fluid to the process chamber.
Many of these process fluids must be maintained within a specific temperature range while flowing through the fluid lines to prevent deposits along the path. Also, many of these process fluids are toxic, pyrophoric, corrosive, or otherwise hazardous, so special safeguards must be employed to prevent leakage of the process fluids into the ambient air.
Those process fluids that must be maintained within a particular temperature range while flowing through the fluid lines, may need to be in a gaseous state in order to flow properly through the fluid lines or to enter the process chamber in the proper concentration or condition for processing. Condensation of the process fluids may cause a loss of controllability or repeatability of the process, including a loss of accurate delivery of the process fluid from one wafer to the next or a loss of control over the amount of material deposited on a single wafer. Thus, these process fluids must be maintained above their vaporization temperature, so that they remain gaseous. Additionally, many of these process fluids are molecular compounds which may decompose, or chemically breakdown into their constituent elements or other molecules, above a certain temperature. Thus, these process fluids must be maintained below their decomposition temperature.
Some of these process fluids may have a fairly wide window between their vaporization temperature and their decomposition temperature, so that maintaining the fluid lines and the process fluid within the required temperature range may be fairly easy. Other process fluids, however, may have a narrow window between their vaporization temperature and their decomposition temperature, so that maintaining the fluid lines and the process fluid within the required temperature range may require a very tightly controlled delivery process in order to ensure that the temperature of the entire fluid delivery line does not vary. For example, cupraselect has a vaporization temperature of about 75° C. and a decomposition temperature of about 85° C. Thus, cupraselect has a very narrow temperature range within which it must be maintained for proper operation of a process that uses cupraselect. By comparison, DMAH has a vaporization temperature of about 40° C. and a decomposition temperature of about 180-200° C., and TDMAT has a vaporization temperature of about 50° C. and a decomposition temperature greater than about 300° C. Thus, these compounds present a fairly wide temperature range which is considerably less difficult to maintain than that of cupraselect.
FIG. 1
a
shows a simplified schematic of a process fluid source
10
, a process chamber
12
and the delivery system in between. The fluid delivery system heats the process fluid in a hot box
14
next to the source
10
prior to flowing the process fluid through the fluid lines
16
to the process chamber
12
. One or more fluid lines (not shown) are attached to the process fluid source
10
and connected to a system of valves (not shown) for regulating the flow of the process fluid. These fluid lines and valves are typically housed within the hot box
14
. The hot box
14
is a closed heated environment for heating the regulating valves and the fluid lines that are immediately adjacent to the fluid source
10
. Thus, the process fluid enters the fluid lines
16
for delivery to the process chamber
12
within the appropriate temperature range. The hot box
14
does not heat the fluid lines
16
that deliver the process fluid to the process chamber
12
.
Since there may be several feet of fluid delivery line between the process fluid source and the process chamber, the fluid delivery line may also have to be heated. Otherwise, the process fluid may condense within the fluid lines before it reaches the process chamber and disrupt the proper functioning of the process.
FIG. 1
b
shows a portion of a fluid delivery line
16
illustrating the means for heating the fluid line
16
between the hot box
14
and the process chamber
12
. The fluid line
16
has an angled portion
18
and a section
20
that does not have the same diameter as the rest of the fluid line
16
. Section
20
may be a fitting or a joint connecting two portions of the fluid line
16
, or a valve section controlling the flow through the fluid line
16
, or an intersection of more than one fluid line
16
, or some other line section disp
Applied Materials Inc.
Campbell Thor
Moser Patterson & Sheridan
Walberg Teresa
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