Stock material or miscellaneous articles – Structurally defined web or sheet – Continuous and nonuniform or irregular surface on layer or...
Patent
1987-01-07
1989-06-06
Lesmes, George F.
Stock material or miscellaneous articles
Structurally defined web or sheet
Continuous and nonuniform or irregular surface on layer or...
106442, 106401, 350105, 404 14, 423600, 423625, 423628, 428141, 428329, 428402, 428457, 501127, 523172, C01F 702, F21D 722, B32B 903
Patent
active
048370690
ABSTRACT:
Procedure for making Al.sub.2 O.sub.3 spheroids, 600 micrometers in diameter or less, utilizes an AlOOH sol containing 0.25% weight percent MgO (in the form of Mg(NO.sub.3).sub.2 .multidot.6H.sub.2 O) and HNO.sub.3. The sol is dispersed into droplets in a particle forming fluid (e.g., 2-ethylhexanol) where gelling occurs. The gelled spheroids are collected, dried and pre-fired in air at temperatures less than 1,200.degree. C. for up to about 12 hours. The dried and prefired beads are fired in a 2-step process at temperatures of about 1,850-1,950.degree. C. in the following sequence:
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Bescup Terrance L.
Fellows Benjamin T.
Leedecke Charles J.
Kirn Walter N.
Lesmes George F.
Little Douglas B.
Minnesota Mining and Manufacturing Company
Monroe James B.
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