Transparent alumina microspheres

Stock material or miscellaneous articles – Structurally defined web or sheet – Continuous and nonuniform or irregular surface on layer or...

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106442, 106401, 350105, 404 14, 423600, 423625, 423628, 428141, 428329, 428402, 428457, 501127, 523172, C01F 702, F21D 722, B32B 903

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048370690

ABSTRACT:
Procedure for making Al.sub.2 O.sub.3 spheroids, 600 micrometers in diameter or less, utilizes an AlOOH sol containing 0.25% weight percent MgO (in the form of Mg(NO.sub.3).sub.2 .multidot.6H.sub.2 O) and HNO.sub.3. The sol is dispersed into droplets in a particle forming fluid (e.g., 2-ethylhexanol) where gelling occurs. The gelled spheroids are collected, dried and pre-fired in air at temperatures less than 1,200.degree. C. for up to about 12 hours. The dried and prefired beads are fired in a 2-step process at temperatures of about 1,850-1,950.degree. C. in the following sequence:

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