Toluene diisocyanate residue

Organic compounds -- part of the class 532-570 series – Organic compounds – Isocyanate esters

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Details

560351, C07C26320

Patent

active

053490827

ABSTRACT:
Disclosed herein is a process for recovering toluene diisocyanate (TDI) from a TDI residue solution, comprising mixing the residue solution with a polyisocyanate consisting essentially of methylenediphenyl diisocyanate (MDI) or MDI in combination with its higher ring oligomer, followed by heating the resulting mixture over a temperature range of 130.degree. to 250.degree. C. for a period of time sufficient to remove free TDI and thermally splittable TDI generated from equilibration of the TDI residue with MDI or the MDI oligomer by either a batch or continuous process.

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patent: 4289589 (1981-09-01), Koehler et al.
patent: 4311800 (1982-01-01), Reischl
patent: 4910333 (1990-03-01), Slack
patent: 5198522 (1993-03-01), Steppan et al.

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