Specialized metallurgical processes – compositions for use therei – Processes – Producing or purifying free metal powder or producing or...
Patent
1994-05-19
1995-08-22
Rosenberg, Peter D.
Specialized metallurgical processes, compositions for use therei
Processes
Producing or purifying free metal powder or producing or...
B22F 900
Patent
active
054429781
ABSTRACT:
Fine tantalum powder of high surface area, high capacitance, low leakage and high breakdown voltage is produced by sodium reduction of highly dilute fluotantalate salt charges at high reaction temperatures and stepwise additions of the sodium reducing agent in a time-series of substantially even weight slugs added over the whole course of the reduction reaction to a melt of the charge and using the small exotherm of reduction provided by each slug as a temperature control factor.
REFERENCES:
patent: 2950185 (1960-08-01), Hellier
patent: 4149876 (1979-04-01), Rerat
patent: 4684399 (1987-08-01), Bergman
patent: 4725312 (1988-02-01), Seon
Gibbons Leo G.
Hildreth Richard
Shaw Malcolm
Tripp Terrance B.
Cohen Jerry
H. C. Starck Inc.
Rosenberg Peter D.
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