Scanning electron microscope fiber push-out apparatus and method

Radiant energy – Inspection of solids or liquids by charged particles

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

250307, 250310, 73842, H01J 3728

Patent

active

055593291

ABSTRACT:
The application discloses an apparatus for measuring interfacial properties of a fiber-matrix composite material, such as a ceramic-matrix, metal-matrix or continuous fiber metal-matrix composite; or a support material, such as a fiber-optic fiber support medium. The apparatus includes a linear motion feedthrough having an indentor for pushing a fiber end, a load cell for sensing debonding and frictional sliding loads, and a scanning electron microscope (SEM) for magnifying the material in order to align the indentor with the fiber end. The feedthrough may push the fiber at a predetermined velocity with up to about a 20 pound load force. The SEM may include a vacuum chamber for housing the material, the indentor, the load cell, and a hot stage module. The hot stage module may increase the temperature of the material to about 1500.degree. C. The apparatus may also include a data acquisition computer for recording the force with respect to time as the fiber is pushed out of the matrix, an acoustic sensor for recording a time when the fiber is debonded from the matrix, and an imaging computer for recording an image of the material. Alternatively, an apparatus may measure a bending or a crushing force which is applied to a fiber shaft by an indentor. Alternatively, a method may sense interfacial properties of a composite material including a plurality of fibers in a matrix having a diameter less than about 10 .mu.m.

REFERENCES:
patent: 4632864 (1986-12-01), Cordova et al.
patent: 4662228 (1987-05-01), Tse
patent: 4848141 (1989-07-01), Oliver et al.
patent: 4972720 (1990-11-01), Wu
patent: 5361641 (1994-11-01), Eldridge et al.
Continuous Ceramic Fiber Aluminum Matrix Composites, pp. 1-6, 3M.
J. I. Eldridge et al., Fiber Push-out Testing Apparatus for Elevated Temperatures, pp. 1035-1042, Apr. 1994, J. Mater. Res., vol. 9, No. 4.
A. M. Daniel et al., A Scanning Electron Microscope Based Microindentation System, pp. 632-638, Mar. 1994, Rev. Sci. Instrum., vol. 85, No. 3.
The Nano Indenter.TM. II, pp. 1-6, Nano.TM. Instruments, Inc.
G. M. Pharr et al., Measurement of Thin Film Mechanical Properties Using Nanoindentation, pp. 28-33, Jul. 1992, Materials Research Society Bulletin, vol. 17, No. 7.
W. C. Oliver et al., An Improved Technique for Determining Hardness and Elastic Modulus Using Load and Displacement Sensing Indentation Experiments, pp. 1564-1583, Jun. 1992, J. Mater. Res., vol. 7, No. 6.
D. B. Marshall et al., Measurement of Interfacial Debonding and Sliding Resistance in Fiber Reinforced Intermetallics, pp. 443-454, 1992, Acta metall. mater., vol. 40, No. 3.
J. I. Eldridge, Desktop Fiber Push-Out Apparatus, pp. 1-11, Dec. 1991, NASA Technical Memorandum 105341.
P. D. Jero et al., Effect of Interfacial Roughness on the Frictional Stress Measured Using Pushout Tests, pp. 1-9, Nov. 1991, Journal of the American Ceramic Society, vol. 74, No. 11.
T. P. Weihs et al., Experimental Examination of the Push-Down Technique for Measuring the Sending Resistance of Silicon Carbide Fibers in a Ceramic Matrix, pp. 524-534, Mar. 1991, Journal of the American Ceramic Society, vol. 74, No. 3.
J. D. Bright et al., Interfacial Sliding Friction in Silicon Carbide-Borosilicate Glass Composites: A Comparison of Pullout and Pushout Tests, pp. 115-122, Jan. 1991, Journal of the American Ceramic Society, vol. 74, No. 1.
G. Morscher et al., Temperature Dependence of Interfacial Shear Strength in SiC-Fiber-Reinforced Reaction-Bonded Silicon Nitride, pp. 713-718, Mar. 1990, Journal of the American Ceramic Society, vol. 73, No. 3.
D. C. Cranmer et al., Comparison of Methods for Determining Fiber/Matrix Interface Frictional Stresses in Ceramic Matrix Composites, pp. 124-135, 1990, ASTM STP 1080.
D. B. Marshall et al., An Indentation Method for Measuring Residual Stresses in Fiber-reinforced Ceramics, pp. 95-103, 1990, Materials Science and Engineering, A126.
J. D. Bright et al., Interfacial Bonding and Friction in Silicon Carbide (Filament)-Reinforced Ceramic-and Glass-Matrix Composites, pp. 1891-1898, Oct. 1989, Journal of the American Ceramic Society, vol. 72, No. 10.
D. B. Marshal et al., Measurement of Interfacial Mechanical Properties in Fiber-Reinforced Ceramic Composites, pp. 542-548, Aug. 1987, Journal of the American Ceramic Society, vol. 70, No. 8.
P. D. Warren et al., Design, Analysis and Application of An Improved Push-through Test for the Measurement of Interface Properties in Composites, pp. 1-30, Materials, University of California.
D. B. Marshal et al., Interfacial Properties and Residual Stresses in Titanium and Titanium Aluminide Matrix Composites, pp. 1-19, Rockwell International Science Center.
T. W. Clyne et al., Interfacial Mechanical Testing of Metal Matrix Composites, pp. 127-139, University of Cambridge.
M. H. Lewis et al., Microstructure-property Relationships in Silicate-matrix Composites, pp. 109-118, Journal of Microscopy, vol. 169, Pt. 2, Feb. 1993.
A. M. Daniel et al., Measurement of Interfacial Micromechanics in Fibre Reinforced Ceramic Matrix Composites, pp. 131-138, Ceram. Eng. Sci. Proc. 14, Jul.-Aug., 1993.
M. H. Lewis et al., Microstructure and Macromechanical Behaviour of CMC's, pp. 10-1-10-13, Introduction of Ceramics into Aerospace Structural Composites, Proceedings of the AGARD/NATO Workshop, Apr. 1993.
M. G. Cain et al., Presynthesised Interfaces for Ceramic Matrix Composites via Fibre Coating, pp. 246-252, Materials Letters, vol. 17, No. 5, Sep. 1993.
A. M. Daniel et al., Measurement of Interfacial Micromechanics in Ceramic Matrix Composites, pp. 108-113, British Ceramic Transactions, vol. 93, No. 3, Mar. 1994.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Scanning electron microscope fiber push-out apparatus and method does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Scanning electron microscope fiber push-out apparatus and method, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Scanning electron microscope fiber push-out apparatus and method will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-1930364

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.