Process for the synthesis of acetic acid, (dimethoxyphosphinyl)

Details Process for the synthesis of acetic acid, (dimethoxyphosphinyl) Process for the synthesis of acetic acid, (dimethoxyphosphinyl)

1993-04-28

1994-02-22

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Silicon containing

C07F 708, C07F 718

Patent

active

052888886

ABSTRACT:
The invention is an improved process for the large scale production of acetic acid, (dimethoxyphosphinyl) [[1,1-dimethylethyl)dimethylsilyl]oxy]-, (4-nitrophenyl)methyl ester.

REFERENCES:
patent: 4804770 (1989-02-01), Karanewsky
patent: 4992429 (1991-02-01), Ulrich et al.
patent: 5017716 (1991-05-01), Karanewsky et al.
patent: 5210110 (1993-05-01), Rutsch et al.
D. Horne, J. Gaudino, and W. J. Thompson, Tetrahedron Letters, vol. 25, No. 33, 3529-3532, Apr. 1984; "A Method for the Synthesis of .alpha.-Ketoesters from Aldehydes".
E. Nakamura, Tetrahedron Letters, vol. 22, 663-666, Jun. 1981; "New Acyl Anion Equivalent".
F. Texier-Boullet and A. Foucaud, Synthesis, 916, Sep. 1982; "Synthesis of 1-Hydroxyalkanephosphonic Esters on Alumina".

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