Process for the stabilizing of an organosilane

Organic compounds -- part of the class 532-570 series – Organic compounds – Silicon containing

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556440, 564434, 564437, C07C20984, C07F 708

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059455543

ABSTRACT:
A process for the stabilizing of an organosilane with an effective, stabilizing amount of purified N,N'-diphenyl-p-phenylenediamine (DPPD). The purification of crude DPPD involves extracting crude DPPD with hexane thereby forming an extract solution containing DPPD, passing the extract solution over an adsorption layer comprising silica gel as the adsorbent to form a solution containing purified DPPD and recovering the purified DPPD from the solution.

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patent: 2833824 (1958-05-01), Pecherer
patent: 4946977 (1990-08-01), Bernhardt et al.
patent: 5763666 (1998-06-01), Frings et al.
Chemical Abstracts, vol. 89, No. 3, Jul. 17, 1978, AN-23925, S. I. Burmistrov, et al., "Purification of N,N'-Dephenyl-P-Phenylenediamine", and SU 595 295, Mar. 20, 1978.
Beilstein 13, IV, p. 116.
Chemical Abstracts, vol. 67, Abstract No. 3353m, Jul. 3, 1967.
The Merck Index, p. 389, 1968.

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