Process for the pulping of lignocellulose materials with alkali

Paper making and fiber liberation – Processes of chemical liberation – recovery or purification... – With squeezing – compression – rubbing – kneading

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162 72, 162 77, 162 90, D21C 302, D21C 320

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047909056

ABSTRACT:
A process for preparing a cellulose paste by treatment of lignocellulose materials which comprises impregnating wood or vegetable shavings in divided form with an aqueous solution containing 2 to 20% by weight of alkaline metal hydroxides, alkali metal salts, or alkaline earth metal hydroxides, adjusting the weight of the solution retained by impregnation to a value representing 1 to 3 times the weight of treated material, the ratio of the weight of the impregnated mass to the dry weight of the lignocellulosic material being preferably not more than about 2.6:1, subjecting the impregnated masses to cooking treatment by exclusively indirect heating at a temperature varying from 150.degree. to 200.degree. C. without exerting any mechanical disintegrating action for a period varying from 15 to 60 minutes, and pressing the cooked product so as to extract therefrom the solubilized lignin in the form of a black liquor containing about 50% of dry material. When operating at atmospheric pressure, the aqueous solution may further contain from 2 to 20% by weight of solvent chosen from the group comprising glycols, alkanolamines, sulfoxides and fatty acid salts.

REFERENCES:
patent: 2218479 (1940-10-01), Peterson et al.
patent: 3255071 (1966-06-01), Kleinert
patent: 3664918 (1972-05-01), Clayton
patent: 4091749 (1978-05-01), Procter et al.
patent: 4248663 (1981-02-01), Kubes
patent: 4552616 (1985-11-01), Kauppi
Rydhulm, "Pulping Processes", Interscience Publishers, N. Y., 1969, p. 336.

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