Process for the production of sintered aluminum nitrides

Compositions: ceramic – Ceramic compositions – Refractory

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501 98, 501153, 264 65, 264 66, C04B 3558, C04B 3564

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active

047787783

ABSTRACT:
Process for producing sintered aluminum nitride bodies, comprising sintering a relatively impure aluminum nitride powder comprising at least 95% by weight aluminum nitride and having no more than 3% bound oxygen content, no more than 0.6% metal or metal compound impurities, and no more than 0.5% silicon or carbon impurities, the sintering being carried out by heating the aluminum nitride body from room temperature to the sintering temperature at a rate of no more than 250.degree. C. per hour; introducing an inert gas containing from 1 to 4% by volume hydrogen until the temperature reaches 1200.degree. C.; continuing to introduce solely an inert gas as the temperature is further increased to the sintering temperature; sintering the body at a sintering temperature of from 1600.degree. to 1900.degree. C.; and cooling the sintered body at a rate of no more than 300.degree. C. per hour.

REFERENCES:
patent: 3108887 (1963-10-01), Lenie et al.
patent: 3930787 (1976-01-01), DeHollander et al.
patent: 4350651 (1982-09-01), Morell et al.
patent: 4547471 (1985-10-01), Huseby et al.
patent: 4618592 (1986-10-01), Kuramoto et al.

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