Process for the preparation of nitric esters of monohydric...

Details Process for the preparation of nitric esters of monohydric... Process for the preparation of nitric esters of monohydric...

2006-11-20

2009-12-15

Sullivan, Daniel M (Department: 1621)

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitrate esters or chalcogen analogues thereof

C558S483000

Reexamination Certificate

active

07632960

ABSTRACT:
The present invention relates to a process for the preparation of nitric esters of monohydric alcohols wherein a monohydric alcohol or a mixture of monohydric alcohols is converted with nitric acid to the corresponding nitric esters under adiabatic reaction conditions in the presence of sulfuric acid.

REFERENCES:
patent: 2618650 (1952-11-01), Hinkamp et al.
patent: 2734910 (1956-02-01), Himkamp et al.
patent: 2768964 (1956-10-01), Spaeth
patent: 4021498 (1977-05-01), Alexanderson et al.
patent: 4091042 (1978-05-01), Alexanderson et al.
patent: 4479905 (1984-10-01), Knapp et al.
patent: 4496782 (1985-01-01), Carr
patent: 1034603 (1978-07-01), None
R.Andreozzi, R.Marotta, R.Sanchirico, Thermal decomposition of acetic anhydride-nitric acid mixtures, Journal of Hazardous Materials A90, 2002, 111-121.
Römpp Chemielexikon, 10thEd. Georg Thieme Verlag, Shuttgart/ New York, headword: “Cetan-Zahl” (acetane number), p. 649.
Römpp Chemielexikon, 10thEd. Georg Thieme Verlag, Shuttgart/ New York, headwords: “Nitrierung” (nitration); “Nitriersäuer” (nitrating acid) , pp. 2914, 2915 (1998).
Römpp Chemielexikon, 10thEd. vol. 2, Georg Thieme Verlag, Shuttgart/ New York, headword: “Extraktion” (extraction), p. 1268 (1997).
A.B. Quakenbusch and B.T. Pennington, “The Olin Dinitrotoluene (DNT) Process”, Polyurethanes World Congress, pp. 484-488, Oct. 10-13, (1993).
“Extraction liquid-liquid”, Kirk-Othmer, Encyclopedia of Chemical Terminology, 3rdEd. vol. 9, John Wiley & Sons, pp. 672-716, (1980).
Health Hazard Evaluation Report No. HETA 82-285-1339, in Chem. Abstracts 102, 190181, 21 pgs., (1985).

Affiliated with

Also associated with

Rating

Process for the preparation of nitric esters of monohydric... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for the preparation of nitric esters of monohydric..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for the preparation of nitric esters of monohydric... will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFUS-PAI-O-4130200