Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1978-04-19
1980-09-09
Niebling, John F.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
2604124, 2604128, 2601235, A23J 700, C07F 902, C11C 300
Patent
active
042217318
ABSTRACT:
A method of recovering a high-grade lecithin and solvents from an oil-bearing full miscella which also contains lecithin and which results from an oilseed ternary solvent extraction process. The method may include a first step of phase separation of the oil-bearing miscella containing lecithin and the ternary solvents into a polar and a non-polar phase, and a second step of azeotropic distillation of the non-polar phase to recover a portion of the solvents, and to remove substantially all the water from the residual crude oil, thereby keeping the lecithin in solution. A commercial grade lecithin having good water dispersibility is subsequently recovered from the residual crude oil, and a small amount of highly water dispersible lecithin may be recovered from the polar phase by atmospheric distillation.
In another embodiment, when the full miscella containing crude oil ternary solvent and lecithin resulting from the above ternary solvent extraction is initially subjected to azeotropic distillation to recover solvent therefrom and remove substantially all the water, a highly water dispersible lecithin having a high choline chloride content is obtained. Premature degumming of this highly water dispersible lecithin is avoided by maintaining the solvent ratios above certain minimums.
The ternary solvents for the oilseed extraction include a lipophilic hydrocarbon, such as hexane; a water miscible lower alcohol, such as ethanol; and a minor amount of water. The recovery method is energy efficient, because the boiling temperature of the ternary azeotrope is lower than any other combination of the three solvents.
REFERENCES:
patent: 2615905 (1952-10-01), Heinrich
patent: 3357918 (1967-12-01), Davis
patent: 3714210 (1973-01-01), Schweiger
patent: 3878232 (1975-04-01), Hayes
patent: 3998800 (1976-12-01), Youngquist
Orthoefer Frank T.
Short Robert G.
A. E. Staley Manufacturing Company
Hendrickson M. Paul
Meyerson Charles J.
Niebling John F.
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