Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing
Patent
1980-01-18
1981-03-17
Hearn, Brian E.
Organic compounds -- part of the class 532-570 series
Organic compounds
Amino nitrogen containing
C07C12600
Patent
active
042566622
ABSTRACT:
Urea is synthesized from ammonia and carbon dioxide at increased pressure and elevated temperature. The unconverted starting components are separated and recycled to the synthesis stage and the resulting urea solution is vacuum thickened. The liquor vapor resulting from the vacuum-thickening is condensed under a pressure of from 0.04 to 0.90 ata by means of indirect cooling water, followed by contacting the uncondensed liquor vapor with an aqueous solution of the unconverted starting feed at a temperature of from 10.degree. to 60.degree. C. and pressure of from 1.5 to 18 ata for subsequent absorption condensation. The process according to the present invention makes it possible to reduce the rate of consumption of steam (per ton of urea) by 0.1-0.25 t/t and the rate of consumption of the cooling return water by 6 to 14 m.sup.3 /t.
REFERENCES:
patent: 3317601 (1967-05-01), Otsuka
patent: 3922222 (1975-11-01), Van Moorsel
patent: 4053507 (1977-10-01), Inoue
Chemical Abstracts, vol. 78 (1973), Nos. 3754v, 3755w.
Weyermuller et al., "Dutch Urea Process", Chemical Processing, 9/24/62, pp. 19-23.
Gorlovsky David M.
Korshunov Petr E.
Kucheryavy Vladimir I.
Lebedev Vladimir V.
Pikhtovnikov Boris I.
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