Process for producing phosphate

Organic compounds -- part of the class 532-570 series – Organic compounds – Phosphorus esters

Reexamination Certificate

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Details

C558S104000

Reexamination Certificate

active

07541484

ABSTRACT:
The invention relates to a process for producing a phosphate, which includes reacting a phosphorus pentaoxide-containing phosphorylating agent with an organic hydroxy compound, the reaction being carried out at a reaction temperature of 50 to 70° C. until the degree (w) of remaining phosphorus pentaoxide undissolved in a reaction solution, defined by the following equation (1), is reduced to 15 wt % or less:in-line-formulae description="In-line Formulae" end="lead"?W=[1−(AVt−AVp)/AV0]×100  (1)in-line-formulae description="In-line Formulae" end="tail"?wherein W is the degree [wt %] of remaining phosphorus pentaoxide undissolved in a reaction solution; AVtis the acid value [mg KOH/g] of the reaction solution excluding undissolved phosphorus pentaoxide in an arbitrary time; AVpis the theoretical acid value [mg KOH/g] of the phosphorylating agent excluding undissolved phosphorus pentaoxide; and AV0is the theoretical acid value [mg KOH/g] of phosphorus pentaoxide.

REFERENCES:
patent: 2003/0065205 (2003-04-01), Tsuyutani et al.
patent: 1 435 358 (2004-07-01), None
patent: 38-12524 (1963-07-01), None
patent: 60-43076 (1985-09-01), None
patent: 62-25155 (1987-06-01), None
patent: 3-27558 (1991-04-01), None
patent: 5-66958 (1993-09-01), None
patent: 11-158193 (1999-06-01), None

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