Process for producing hexachlorodisilane

Chemistry of inorganic compounds – Silicon or compound thereof – Halogen containing

Reexamination Certificate

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C423S350000, C203S029000

Reexamination Certificate

active

06846473

ABSTRACT:
A process for producing hexachlorodisilane comprising, condensing an exhaust gas discharged from a reactor for producing polycrystalline silicon from a chlorosilane and hydrogen to separate the hydrogen, distilling the resultant condensate to separate the unreacted chlorosilane and by-product silicon tetrachloride, and then further distilling to recover hexachlorodisilane, wherein tetrachlorodisilane can be recovered together with the hexachlorodisilane, and the hexachlorodisilane and tetrachlorodisilane recovered have a far higher purity than the conventional ones produced from metallic silicon.

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