Process for preparing vegetable oil fractions rich in...

Food or edible material: processes – compositions – and products – Products per se – or processes of preparing or treating... – Fat or oil is basic ingredient other than butter in emulsion...

Reexamination Certificate

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C426S002000, C426S601000, C424S439000, C514S141000, C514S211070

Reexamination Certificate

active

10451457

ABSTRACT:
A vegetable oil fraction rich in non-tocolic, high-melting, unsaponifiable matter is prepared by the following steps: A vegetable oil having a slip melting point of not more thatn 30° C. and a content of unsaponifiable matter of at least 0.5% by weight is hydrogenated to fully saturate the fatty acids of the glycerides and to reach a slip melting point of at least 57° C. To the hydrogenated oil is added from 1 to 75% by weight of the unhydrogenated starting oil or another oil having a slip melting point of not more than 30° C. in order to act as a carrier and vehicle for the unsaponifiable matter. Then, a solvent is added to the oil mixture in a ratio between oil and solvent from 1:2 to 1:20, and the mixture is heated to transparency. The oil/-solvent-mixture is cooled in one or more steps to a final temperature in the range from −35 to +30° C., and the precipitated high-melting fraction(s) is (are) filtered off. The filtrate is desolventised, leaving a fraction rich in unsaponifiable matter. By this process very high concentrations of in particular the non-tocolic, higher melting unsaponifiables can be achieved, and the composition of the glyceridic part of the enriched fraction can betailored to specific applications. Also, a novel blood cholesterol-lowering effect of the unsaponifiable constituents from shea butter has been found.

REFERENCES:
patent: 5679393 (1997-10-01), Laur et al.
patent: 0 690 904 (1997-06-01), None
Swern, D, ed. 1979. Bailey's Industrial Oil and Fat Products, vol. 1, 4th edition. John Wiley & Sons, New York, p. 192-196. 323, 328.
Firestone, ed. 1999. Physical and Chemical Characteristics of Oils, Fats and Waxes. AOCS Press, Champaign, III, p. 92.
Turpin, P.E., “The Fractionation of Shea Nut Oil . . . ”, Fat Sci. Tech., 92, Nr. 5, 1990, pp. 179-184.

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