Process for preparing N,N-dimethyl 2-(methylthio) benzamides and

Details Process for preparing N,N-dimethyl 2-(methylthio) benzamides and Process for preparing N,N-dimethyl 2-(methylthio) benzamides and

1987-12-28

1989-03-21

Lieberman, Paul

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

564134, 546298, C07C14941, C07C10206, C07D21362

Patent

active

048145017

ABSTRACT:
Pyrolysis of substituted salicylate O(N,N-dialkyl)thiocarbamates yielded the corresponding N,N-dialkyl-2-(methylthio)benzamide. Similarly, substituted 6-azasalicylate O(N,N-dialkyl)thiocarbamates yielded the corresponding N,N-dialkyl-2-(methylthio)-6-aza-benzamide.

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patent: 3878225 (1975-04-01), Allen et al.
patent: 3980659 (1976-09-01), Fleckenstein et al.
Newman, M. S. and Karnes, H. A., J. Org. Chem., 31, 3980 (1966).
Muchowski, J. M., et al. J. Med. Chem., 28, (8), 1037 (1985).
Carral, C. et al, Synthesis 172 (1984).

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