Process for extracting lignin from lignocellulosic material usin

Paper making and fiber liberation – Processes of chemical liberation – recovery or purification... – Treatment with particular chemical

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162 77, 162 90, D21C 320

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active

047464011

ABSTRACT:
A process for the delignification of cellulosic materials, wherein a high-yield cellulose pulp and high-value by-product, such as reactive lignins of low molecular weight are produced, which comprises degassing lignocellulosic material, rapidly heating the lignocellulosic material in a liquor comprising water, an organic solvent and a buffer thereby maintaining a substantially neutral solvent extraction, such that said lignocellulosic material is cooked in the liquor as it is heated from a temperature of 150.degree. C. to a selected maximum temperature in the range of 200.degree. to 280.degree. C.; and rapidly cooling the mixture to a temperature less than 150.degree. C. The reaction is controlled to maximize reactive lignin solvation while suppressing cellulose degradation.

REFERENCES:
patent: 2037001 (1981-07-01), Aronovsky
patent: 4496426 (1985-01-01), Baumeister et al.
patent: 4520105 (1985-05-01), Sinner et al.
patent: 4597830 (1986-07-01), April et al.
Rydholm "Pulping Processes"; Int. Publishers, pp. 300-305, 1969.

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