Process for crystal growth from solution

Adhesive bonding and miscellaneous chemical manufacture – Delaminating processes adapted for specified product – Delaminating in preparation for post processing recycling step

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156621, 156622, 156624, 156DIG63, 156DIG71, 156DIG78, 156DIG86, 156DIG87, 156DIG89, C30B 708, C30B 710

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047938943

ABSTRACT:
A method of producing large flow-free single crystals of either LiNdP.sub.4 O.sub.12 or XB.sub.2 O.sub.4, where X is Ba, Sr or Ca, comprising the steps of, preparing a mixture of the final product and a flux of oxide of their precursors, melting the mixture, fluxing at a temperature substantially equal to the saturation value then suspending a seed in the melt, and cooling while maintaining essentially spatially isothermal conditions throughout said melt to crystallize single crystals on the seed.

REFERENCES:
patent: 4000247 (1976-12-01), Yamada et al.
patent: 4082601 (1978-04-01), Regreny et al.
patent: 4500397 (1985-02-01), Mori
Nakano et al., Crystal Defects in Laser Material LiNdP.sub.4 O.sub.12, Journal of Crystal Growth 53 (1981) pp. 375-381.
Jiang et al., Flux Growth of Large Single Crystals of Low Temperature Phase Barium Metaborate, Journal of Crystal Growth, 79 (1986) 963-969.

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