Preparation of sputtering targets

Chemistry: electrical and wave energy – Processes and products – Coating – forming or etching by sputtering

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2041921, 20419215, 20429813, 156 89, 264 61, 264212, C23C 1434, C03B 2900, C04B 3334, B29D 700

Patent

active

057097836

ABSTRACT:
Method for preparing sputtering targets according to one embodiment, by reacting a mixture of alkoxides of metals such as titanium, lanthanum and zirconium, with a soluble lead compound such as lead acetate in an organic solvent in the presence of aqueous ammonium hydroxide, to form a sol-gel. The solvent is removed from the sol-gel to form a powder. The powder is mixed with a liquid medium, e.g. an aqueous medium containing an organosol, to form a slurry of the powder and the slurry is cast on a substrate such as a polyester tape and dried to form a tape of the sol-gel. The tape is cut into individual tapes and the tapes are stacked and laminated under heat and pressure into a monolithic unit, which is then filed at high temperature. The dense monolithic unit thus formed is mechanically machined to the desired shape, e.g. in the form of a circular disc, to produce a sputtering target.

REFERENCES:
patent: 3518756 (1970-07-01), Bennett et al.
patent: 3695960 (1972-10-01), Richter
patent: 5091221 (1992-02-01), Chu et al.
patent: 5162977 (1992-11-01), Paurus et al.
patent: 5507898 (1996-04-01), Aoki et al.
L.E. Sanchez, D.T. Dionk, S.Y. Wu, and I.K. Naik; "Processing And Characterization of Sol-Gel Derived Very Thin Film Ferroelectric Capacitors"; Ferroelectrics, 1991, vol. 116, pp. 1-17.

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