Precleaning method of precleaning a silicon nitride film...

Semiconductor device manufacturing: process – Coating of substrate containing semiconductor region or of... – Insulative material deposited upon semiconductive substrate

Reexamination Certificate

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C438S775000, C438S778000, C438S905000

Reexamination Certificate

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06844273

ABSTRACT:
A thermal processing system (1) includes a reaction vessel (2) capable of forming a silicon nitride film on semiconductor wafers (10) through interaction between hexachlorodisilane and ammonia, and an exhaust pipe (16) connected to the reaction vessel (2). The reaction vessel2is heated at a temperature in the range of 500 to 900° C. and the exhaust pipe (16) is heated at 100° C. before disassembling and cleaning the exhaust pipe16. Ammonia is supplied through a process gas supply pipe (13) into the reaction vessel (2), and the ammonia is discharged from the reaction vessel (2) into the exhaust pipe (16).

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Tanaka et al. “Film Properties of Low-k Silicon Nitride Films Formed by Hexachlorodisilane and Ammonia”, 2000, Journal of The Electrochemical Society, pp. 2284-2289.

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