Micro-patterned SiO 2 /TiO 2 films through photo and...

Radiation imagery chemistry: process – composition – or product th – Imaging affecting physical property of radiation sensitive...

Reexamination Certificate

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C430S005000, C430S322000

Reexamination Certificate

active

07622239

ABSTRACT:
A method for making a patterned SiO2films over TiO2(Si02/Ti02) under ambient atmospheric conditions, including room temperature, through photo and chemical reactions. The method is simple, convenient and can be performed in a short period of time, typically less than two hours. The patterned TiO2film is fabricated through photo-irradiation of a photosensitive organic-titanium film using a mask. Silica particles are generated from silicate solution by adjusting pH values to 10 to 8 with hydrochloric acid. The pre-deposited TiO2film has a strong attraction for the SiO2particles, leading to the instant formation of SiO2film over the TiO2film. The silica films are also amino-silylated with 3-aminopropyltriethoxysilane toward applications such as patternable, location-specific silica-based separation and purification.

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