Method of synthesizing nitrato alkyl oxetanes

Details Method of synthesizing nitrato alkyl oxetanes Method of synthesizing nitrato alkyl oxetanes

1989-07-10

1993-05-25

Ivy, C. Warren

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

C07D30504

Patent

active

052141667

ABSTRACT:
Nitrato alkyl oxetanes are synthesized directly from the corresponding hyxy alkyl oxetanes by nitrating the hydroxy alkyl oxetane under non-acidic anhydrous conditions. A hydroxy alkyl oxetane is reacted with an anhydrous nitrate ester of a carboxylic acid at temperatures below about 10.degree. C. The product of the method, nitrato alkyl oxetane, is produced in relatively high yield without opening of the oxetane ring.

REFERENCES:
patent: 3932412 (1976-01-01), Simpson
patent: 4431830 (1984-02-01), Schonafinger
patent: 4683086 (1987-07-01), Frankel et al.

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