Method of preparing sulfonimide or its salt

Details Method of preparing sulfonimide or its salt Method of preparing sulfonimide or its salt

1995-09-07

1998-03-03

O'Sullivan, Peter

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

C07C30338

Patent

active

057236640

ABSTRACT:
The invention relates to a method of preparing a sulfonimide, a first salt thereof, or a second salt thereof. The method includes the step of: (a) reacting one or two sulfonyl fluorides with nonhydrous ammonia and an amine component which is one of a tertiary amine and a heterocyclic amine, so as to prepare the first salt. Alternatively, the method includes the step of: (a) reacting the sulfonyl fluoride with the amine component and a sulfonamide, so as to prepare the first salt. The method further optionally includes, after the step (a), the step of: (b) reacting, in an aqueous solution, the first salt with a metal compound, so as to prepare the second salt. The method still further optionally includes, after the step (a), the step of: (c) reacting the first salt with a strong acid so as to prepare the sulfonimide. Alternatively, the method further optionally includes, after the step (b), the step of: (d) reacting the second salt with a strong acid so as to prepare the sulfonimide. The sulfonimide, the first salt or the second salt is easily economically prepared in an industrial scale production with high purity and high yield.

REFERENCES:
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patent: 5256821 (1993-10-01), Armand
patent: 5502251 (1996-03-01), Pohmer
Chemiker-Zeitung, vol. 96, No. 10. 1972, pp. 582-583, XP002019684 J.N. Muessdoerffer et al.
Foropoulos et al. (1984) "Inorganic Chemistry", vol. 23, No. 23, pp. 3720-3723.

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