Method of preparing sulfonimide or its salt

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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C07C30338

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active

057236640

ABSTRACT:
The invention relates to a method of preparing a sulfonimide, a first salt thereof, or a second salt thereof. The method includes the step of: (a) reacting one or two sulfonyl fluorides with nonhydrous ammonia and an amine component which is one of a tertiary amine and a heterocyclic amine, so as to prepare the first salt. Alternatively, the method includes the step of: (a) reacting the sulfonyl fluoride with the amine component and a sulfonamide, so as to prepare the first salt. The method further optionally includes, after the step (a), the step of: (b) reacting, in an aqueous solution, the first salt with a metal compound, so as to prepare the second salt. The method still further optionally includes, after the step (a), the step of: (c) reacting the first salt with a strong acid so as to prepare the sulfonimide. Alternatively, the method further optionally includes, after the step (b), the step of: (d) reacting the second salt with a strong acid so as to prepare the sulfonimide. The sulfonimide, the first salt or the second salt is easily economically prepared in an industrial scale production with high purity and high yield.

REFERENCES:
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patent: 5256821 (1993-10-01), Armand
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Chemiker-Zeitung, vol. 96, No. 10. 1972, pp. 582-583, XP002019684 J.N. Muessdoerffer et al.
Foropoulos et al. (1984) "Inorganic Chemistry", vol. 23, No. 23, pp. 3720-3723.

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