Method of preparing naphthol-modified phenolic resin

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From phenol – phenol ether – or inorganic phenolate

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528129, 528137, 528143, 528155, 525480, 525481, 525501, 525534, C08G 804, C08G 1404

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active

054592232

ABSTRACT:
A naphthol-modified phenolic resin having low softening point and good flowability is obtained by allowing a naphthol and a phenol to react with an aldehyde in the presence of an acid catalyst at 60.degree. to 110.degree. C. to obtain a primary reaction mixture, heating the primary reaction mixture in the presence of a strong acid, a super acid or a mixture thereof under ambient pressure at 120.degree. to 180.degree. C. for 1 to 12 hours to obtain a secondary reaction mixture, and subjecting the secondary reaction mixture to vacuum concentration or steam distillation, and the naphthol-modified phenolic resin is suited to use as a curing agent in epoxy resin molding materials for sealing electronic parts.

REFERENCES:
patent: 3862260 (1975-01-01), Sellers et al.
patent: 4404357 (1983-09-01), Taylor et al.
patent: 4424315 (1984-01-01), Taylor et al.
patent: 5023311 (1991-06-01), Kubota
patent: 5206333 (1993-04-01), Sue et al.
patent: 5302673 (1994-04-01), Naka et al.
Patent Abstracts of Japan, vol. 17, No. 668, 9 Dec. 1993.

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