Method of monitoring and inhibiting scale deposition in pulp...

Paper making and fiber liberation – Processes of chemical liberation – recovery or purification... – With cleaning – preserving or conditioning of apparatus

Reexamination Certificate

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Details

C162S049000, C162S029000, C162S080000, C422S013000

Reexamination Certificate

active

07985318

ABSTRACT:
A method of monitoring and inhibiting scale precipitation and deposition from spent liquor in pulp mill evaporators and concentrators is disclosed. The method includes connecting a black liquor deposition monitor to a pulp mill evaporator or concentrator and measuring the thermal conductivity on the outer surface of the monitor. A controller interprets the measured thermal conductivity and determines a level of scale deposition. If the level of scale deposition is above a predetermined level, the controller is operable to introduce a scale-inhibiting composition to the spent liquor. The scale-inhibiting composition may include organic polycarboxylic acids; organic fatty acids; low molecular weight and polymeric aromatic acids; organic acid esters, anhydrides, and amides; low molecular weight and polymeric aliphatic and aromatic sulfonic acids; and low molecular weight and polymeric amines; and any combinations.

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