Method of measuring oxygen in silicon

Measuring and testing – Gas content of a liquid or a solid – By vibration

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422 80, G01N 3112

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active

048007471

ABSTRACT:
A heat melting type gas extraction apparatus is employed to measure oxygen in a silicon sample. A double graphite crucible is first heated, in the absence of the sample or a flux metal, to extract oxygen therein. The flux metal is then added to the crucible and heated to extract oxygen therein. The sample is then added, melted, and heated to produce a sample gas for analysis.

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patent: 3751965 (1973-08-01), Kraus
patent: 3812705 (1974-05-01), Boillot
patent: 3899627 (1975-08-01), Sitek et al.
patent: 3946228 (1976-03-01), Biermann
patent: 4098576 (1978-07-01), Judge

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