Paper making and fiber liberation – Processes of chemical liberation – recovery or purification... – With chemical or physical modification of liberated fiber
Reexamination Certificate
2001-07-11
2002-07-02
Fortuna, JoséA. (Department: 1731)
Paper making and fiber liberation
Processes of chemical liberation, recovery or purification...
With chemical or physical modification of liberated fiber
C162S181200, C162S181400, C162S158000, C162S183000
Reexamination Certificate
active
06413365
ABSTRACT:
BACKGROUND OF THE INVENTION
1. Field of the Invention.
The present invention relates to an apparatus for loading fibers in a fiber suspension with a chemical compound, and, more particularly, to an apparatus for loading fibers in a fiber suspension with calcium carbonate.
2. Description of the Related Art.
A paper-making machine receives a fiber suspension including a plurality of fibers, such as wood fibers, which are suspended within an aqueous solution. The water is drained and the fiber suspension is dried in the paper-making machine to increase the fiber content and thereby produce a fiber web as an end product.
The fiber web produced by the paper-making machine typically includes organic wood fibers and inorganic fillers. A known inorganic filler is calcium carbonate, which may be added directly to the fiber suspension (direct loaded calcium carbonate). It is also known to chemically load the fibers within a fiber suspension with calcium carbonate in the lumen and walls of the individual fibers (fiber loaded calcium carbonate). The fiber loaded calcium carbonate increases the strength of the paper compared with a direct loaded calcium carbonate (adding calcium carbonate directly to the fiber suspension) at the same loading (filler) level. This yields an economic advantage in that the filler level of the paper is increased by replacing the more expensive fiber source (wood fibers) with calcium carbonate. The finished paper web has higher strength properties due to the increased filler levels of the calcium carbonate. In contrast, the strength properties of a finished web using direct loaded calcium carbonate is less.
For example, U.S. Pat. No. 5,223,090 (Klungness, et al.) discloses a method for chemically loading a fiber suspension with calcium carbonate. In one described method, calcium oxide or calcium hydroxide is placed within a refiner unit and carbon dioxide is injected into the refiner unit at a specified pressure. The fiber suspension is maintained within the refiner for a predetermined period of time to ensure that a proper chemical reaction and thus proper chemical loading of the fiber suspension occurs. In another described method, a fiber suspension with calcium oxide or calcium hydroxide is introduced into a 20 quart food mixer and carbon dioxide gas is injected into the mixer at a specified pressure. Using either the refiner or the food mixer, both methods utilize a batch processing method for processing only a small amount of the fiber suspension at a time. Because of the large amount of fiber suspension which is required at the wet end of a paper-making machine, a batch process requires that the chemically loaded fiber suspension be transferred to another holding tank for ultimate use in a paper-making machine.
What is needed in the a method for chemically loading a fiber suspension for use in a paper-making machine with an adequate output of a chemically loaded fiber suspension, of more than 2,200 cu. ft. up to 132,000 cu. ft. per day for today's paper making process, which allows commercialization of such a chemical loading process.
SUMMARY OF THE INVENTION
The present invention provides a method of loading fibers in a fiber suspension with calcium carbonate using an apparatus having a rotatable distribution member, a rotor and stator assembly, and a toothed ring positioned therein. A reactant gas, such as carbon dioxide, ozone and/or steam, is injected into a gas ring defined between the toothed ring and the rotor and stator assembly so that the chemical reaction forming calcium carbonate occurs.
The invention comprises, in one form thereof, a method of loading fibers in a fiber suspension with calcium carbonate. A fiber suspension is transported to an inlet of a housing. The fiber suspension includes calcium oxide and/or calcium hydroxide. The fiber suspension is distributed from the inlet using a rotatable distribution member. The fiber suspension is passed through a toothed ring interposed between the distribution member and a rotor and stator assembly. A reactant gas is supplied to a gas ring defined between a toothed ring and the rotor and stator assembly. Calcium carbonate crystals are formed in the fiber suspension as the fiber suspension passes through the gas ring. The calcium carbonate crystals are distributed in the fiber suspension using the rotor and stator assembly.
An advantage of the present invention is that the fiber loading of the fiber suspension takes place as a continuous process, thereby providing output quantities of loaded fiber suspension sufficient for use in a paper-making machine.
Another advantage is that the particular type of the calcium carbonate crystals which are formed may be controlled, dependant upon temperature, pH and reaction time within the toothed ring.
Yet another advantage is that the toothed ring controls the flow rate of the fiber suspension through the gas ring.
A still further advantage is that the consistency of the loaded fiber suspension may be varied at the accept outlet using dilution water.
A still further advantage is that loading of the fibers within the fiber suspension occurs in as well as on the fibers.
Another advantage is that the calcium carbonate crystals are generally evenly distributed within the fiber suspension using the rotor and stator assembly.
A still further advantage is that the distribution member as well as the rotor of the rotor and stator assembly are driven by a common input shaft.
Yet another advantage is that since the chemical reaction occurs within the gas ring, the loaded fiber suspension may be discharged to atmospheric pressure for further use or downstream processing.
REFERENCES:
patent: 4892590 (1990-01-01), Gill et al.
patent: 5096539 (1992-03-01), Graham
patent: 5219660 (1993-06-01), Wason et al.
patent: 5223090 (1993-06-01), Klungness et al.
patent: 5244542 (1993-09-01), Bown et al.
patent: 6251222 (2001-06-01), Silenius et al.
patent: 6251356 (2001-06-01), Mathur
Doelle Klaus
Heise Oliver
Fortuna JoseA.
Taylor & Aust P.C.
Voith Paper Patent GmbH
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