Cleaning and liquid contact with solids – Processes – Hollow work – internal surface treatment
Patent
1995-04-26
1997-06-10
Snay, Jeffrey
Cleaning and liquid contact with solids
Processes
Hollow work, internal surface treatment
134 2, 134 3, 134 221, 134 2212, 134 2218, 134 37, 134 42, 438905, B08B 700, B08B 900
Patent
active
056371535
ABSTRACT:
After a polysilicon film is formed on a wafer, a cleaning gas containing ClF.sub.3 at 10 to 50 vol % is supplied into a reaction tube and an exhaust pipe system at a flow rate of 3000 to 3500 SCCM, so as to remove a polysilicon-based film deposited on an inner wall surface of the reaction tube, the surface of a member incorporated in the reaction tube, and an inner wall surface of the exhaust pipe system while the film forming process, by etching using ClF.sub.3. The cleaning gas is supplied while the temperature in the reaction tube is maintained at 450.degree. C. or higher, and in a pressure condition set at the maintained temperature such that an etching rate of the polysilicon-based film by the cleaning gas is higher than an etching rate of silicon which is the material of the reaction tube or the member incorporated in the reaction tube.
REFERENCES:
patent: 5294262 (1994-03-01), Nishimura
patent: 5380370 (1995-01-01), Niino et al.
Fujita Yoshiyuki
Imamura Yasuo
Kato Hitoshi
Lee Hideki
Mikata Yuuichi
Snay Jeffrey
Tokyo Electron Limited
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