Chemistry of inorganic compounds – Treating mixture to obtain metal containing compound – Alkali metal
Patent
1976-01-27
1977-06-28
Vertiz, O. R.
Chemistry of inorganic compounds
Treating mixture to obtain metal containing compound
Alkali metal
423641, C01D
Patent
active
040326152
ABSTRACT:
Alkali metals such as those employed in liquid metal coolant systems can be safely reacted to form hydroxides by first dissolving the alkali metal in relatively inert metals such as lead or bismuth. The alloy thus formed is contacted with a molten salt including the alkali metal hydroxide and possibly the alkali metal carbonate in the presence of oxygen. This oxidizes the alkali metal to an oxide which is soluble within the molten salt. The salt is separated and contacted with steam or steam-CO.sub.2 mixture to convert the alkali metal oxide to the hydroxide. These reactions can be conducted with minimal hydrogen evolution and with the heat of reaction distributed between the several reaction steps.
REFERENCES:
patent: 2202270 (1940-05-01), Scott
patent: 2527443 (1950-10-01), Padgitt
patent: 3134645 (1964-05-01), Szechtman
Jacobson, Encyclopedia of Chemical Reactions, vol. VI, (1956) pp. 257, 353.
Carlson Dean E.
Glenn Hugh W.
Jackson Frank H.
Langel Wayne A.
The United States of America as represented by the United States
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