Method for producing alkyl nitrites and alkyl dinitrites

Details Method for producing alkyl nitrites and alkyl dinitrites Method for producing alkyl nitrites and alkyl dinitrites

2008-01-01

2008-01-01

Saeed, Kamal A. (Department: 1626)

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitrite esters or chalcogen analogues thereof

Reexamination Certificate

active

07314948

ABSTRACT:
In a continuous process for the preparation of alkyl nitrites and dinitrites, an alkanol or dialkanol is first mixed with an aqueous mineral acid, the reaction mixture obtained is then reacted with an inorganic nitrite and the product obtained can then be isolated immediately.

REFERENCES:
patent: 2714606 (1955-08-01), Soloveichik
patent: 3792077 (1974-02-01), Bermes
patent: 4980496 (1990-12-01), Fruchey
patent: 1043310 (1953-03-01), None
patent: WO01/74754 (2001-10-01), None
Noyes, W.A. “n-Butyl Nitrite” Organic Syntheses Collective, vol. 2, 1953, pp. 108-109.
McMurry, John “Organic Chemistry—Fourth Edition” Brooks/Cole Publishing Company, 1996, p. 411.
Organic Syntheses, Noyes, Collective vol. 2 108-109, PY=1953.
Callen et al., Organic Syntheses Coll. vol. 3, pp. 26-28 (1955): “9-Acetylphenanthrene”.

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