Metal treatment – Barrier layer stock material – p-n type
Reexamination Certificate
2006-03-14
2006-03-14
Fourson, George (Department: 2823)
Metal treatment
Barrier layer stock material, p-n type
C257SE23080, C257SE31131, C438S974000
Reexamination Certificate
active
07011717
ABSTRACT:
According to the present invention, there are provided a method for heat treatment of silicon wafers wherein a silicon wafer is subjected to a heat treatment at a temperature of from 1000° C. to the melting point of silicon in an inert gas atmosphere, and temperature decreasing in the heat treatment is performed in an atmosphere containing 1–60% by volume of hydrogen, a method for heat treatment of silicon wafers under a reducing atmosphere containing hydrogen by using a rapid heating and rapid cooling apparatus, wherein temperature decreasing rate from the maximum temperature in the heat treatment to 700° C. is controlled to be 20° C./sec or less, and a silicon wafer which has a crystal defect density of 1.0×104defects/cm3or more in a wafer bulk portion, a crystal defect density of 1.0×104defects/cm3or less in a wafer surface layer of a depth of 0.5 μm from the surface, a crystal defect density of 0.15 defects/cm2or less on a wafer surface and surface roughness of 1.0 nm or less in terms of the P-V value. By these, crystal defects in wafer surface layers can be reduced by a simple method with a small amount of hydrogen used without degrading microroughness of wafers.
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Akiyama Shoji
Kobayashi Norihiro
Matsumoto Yuuichi
Tamatsuka Masaro
Fourson George
García Joannie Adelle
Oliff & Berridg,e PLC
Shin-Etsu Handotai & Co., Ltd.
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