Method and apparatus for identification of crystallographic defe

Radiant energy – Inspection of solids or liquids by charged particles – Methods

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250310, G01N 23203

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active

054669340

ABSTRACT:
An imaging apparatus (10) includes a scanning electron microscope (12) which is controlled to bombard numerous points (62) of a material sample (24) with an electron beam (18). Backscatter diffraction patterns are collected by an image collection system (26) which may include both a slower responding video camera (32) and a faster responding diode array (40). For a baseline point (62), an electron backscatter diffraction pattern collected at the video camera (32) is analyzed to identify representative pixels which reside along Kikuchi bands (78). Backscatter images from subsequent points (62) are rapidly compared (98) with the baseline to detect changes. When changes are not detected, EBSPs are not analyzed. When changes are detected, EBSPs are analyzed to generate new baselines. The resulting collection of analyzed EBSPs are processed (104) to identify microstructure attributes and to characterize defects (64).

REFERENCES:
patent: 4952804 (1990-08-01), Nakagawa et al.
patent: 4990779 (1991-02-01), Yoshitomi et al.
Etingof and Adams; Jun. 6, 1992; Representations of Polycrystalline Microstructure by n-Point Correlation Tensors.
Wright; 1993; A Review of Automated Orientation Imaging Microscopy (OIM).sup.1.
Adams, Wright and Kunze; Apr. 1993; Orientation Imaging: The Emergence of a New Microscopy.
Brent L. Adams; 1993; Orientation Imaging Microscopy: Application to the Measurement of Grain Boundary Structure.

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