Lightweight boron carbide materials with improved mechanical...

Compositions: ceramic – Ceramic compositions – Carbide or oxycarbide containing

Reexamination Certificate

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C501S096400, C501S098400

Reexamination Certificate

active

11174689

ABSTRACT:
This disclosure describes sintered bodies comprising about 90 wt % to about 99 wt % of boron carbide, having a B:C atomic ratio ranging from 3.8 to 4.5:1; 0 to 1 wt % free carbon; 0 to 1 wt % BN or AlN, remainder an oxide binder phase; said sintered body having a uniform microstructure composed of substantially equiaxed grains of said boron carbide; the oxide binder phase comprising at least a rare earth aluminate and optionally Al2O3or other ternary or binary phases of rare earth oxide-alumina systems; the binder phase being present in form of pockets at the multiple grain junctions and the density of no more than 2.6 g/cm3. Also described is a manufacturing process for the above described substantially pore-free, sintered boron carbide materials with high strength and fracture toughness, which can be used for production of large-area parts. This is achieved by liquid phase low temperature-low pressure hot pressing of boron carbide in an argon atmosphere.

REFERENCES:
patent: 4097293 (1978-06-01), Komeya et al.
patent: 5330942 (1994-07-01), Sigl et al.
patent: 5543370 (1996-08-01), Sigl et al.
patent: 2006/0188348 (2006-08-01), Yeckley et al.
patent: 2006/0189474 (2006-08-01), Yeckley et al.

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