Heat switch for chromatographic system and method of operation

Measuring and testing – Gas analysis – Gas chromatography

Reexamination Certificate

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Details

C073S023250, C073S023410

Reexamination Certificate

active

07658092

ABSTRACT:
A heat switch for remote self-contained gas chromatography is disclosed. The device mechanically separates a hot or cold reservoir from the chromatography column when heating or cooling is not needed. The column needs a cooling system to obtain initial temperatures below ambient. At other times the column needs to be heated to relatively high temperatures, during which time the cooling system is preferably detached. The heat switch allows for rapid temperature changes while minimizing the peak cooling power requirement.

REFERENCES:
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patent: 4739654 (1988-04-01), Pilkington et al.
patent: 6029498 (2000-02-01), Walters et al.
patent: 2637685 (1990-04-01), None
patent: 01/73424 (2001-10-01), None
Colwell, J., “The Performance of a Mechanical Heat Switch at Low Temperatures”, The Review of Scientific Instruments, vol. 40, No. 9, Sep. 1969.
Kakac et al., “Heat Conduction” Third Edition, pp. 54, 57-59, Taylor & Francis 1993.
Halliday et al., “Fundamentals of Physics”, Fifth Edition, Chapter 19, Temperature, Heat, and the First Law of Thermodynamics, pp. 470-473, John Wiley & Sons, Inc. 1997.
Phillips et al., “Paraffin-Actuated Heat Switch for Mars Surface Applications”, NASA Tech Brief vol. 26, No. 5 from JPL New Technology Report NPO-30351, May 1, 2002.
Chave et al., “Magnetostrictive Heat Switch for Cryogenic Use”, NASA Tech Brief, Aug. 1999 from http://www.nasatech.com/Briefs/Aug99/NPO20274.html.

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