Food or edible material: processes – compositions – and products – Processes – Extraction utilizing liquid as extracting medium
Reexamination Certificate
2011-05-17
2011-05-17
Heggestad, Helen F (Department: 1789)
Food or edible material: processes, compositions, and products
Processes
Extraction utilizing liquid as extracting medium
C426S431000, C426S434000, C426S472000, C426S478000, C426S481000, C426S506000, C424S725000
Reexamination Certificate
active
07943190
ABSTRACT:
A processing system and methods for extracting phytochemicals from plant materials with subcritical water. The processing system includes a water supply interconnected with a high-pressure pump, diverter valve, a temperature-controllable extraction vessel, a cooler, a pressure-relief valve and a collection apparatus for collecting eluant fractions from the extraction vessel. The processing system controllably varies the temperature of subcritical water within the extraction vessel, and may optionally be configured to controllably vary the pH of subcritical water flowing into the extraction vessel. A plant material is placed into the extraction vessel after which a flow of subcritical water is provided through the extraction vessel for extraction of phytochemicals. The temperature of subcritical water is controllably varied during its flow through the extraction vessel water thereby producing a plurality of eluant subfractions corresponding to the temperature changes, thereby separating the different classes of phytochemicals extracted from the plant material.
REFERENCES:
patent: 4298626 (1981-11-01), Laws et al.
patent: 4490398 (1984-12-01), Behr et al.
patent: 4727889 (1988-03-01), Niven, Jr. et al.
patent: 4898188 (1990-02-01), Niven, Jr. et al.
patent: 5264236 (1993-11-01), Ogasahara et al.
patent: 5705618 (1998-01-01), Westcott et al.
patent: 5925401 (1999-07-01), Kankaanpaa-Anttila et al.
patent: 6001256 (1999-12-01), Hawthorne et al.
patent: 6123945 (2000-09-01), Nakatsu et al.
patent: 6264853 (2001-07-01), Westcott et al.
patent: 6352644 (2002-03-01), Hawthorne et al.
patent: 6458407 (2002-10-01), Miki et al.
patent: 7208181 (2007-04-01), King et al.
patent: 2005/0095332 (2005-05-01), Stanley
patent: 2004/027074 (2004-04-01), None
King, J. W. , “Subcritical Water Extraction of Anthocyanins from Fruit Berry Substrates”, Los Alamos National Laboratory, Los Alamos, NM, Apr., 2006, pp. 1-10.
Eliasson et al., “High-performance liquid chromatographic analysis of secoisolariciresinol diglucoside and hydroxycinnamic acid glucosides in flaxseed by alkaline extraction”, (2003),J. Chromatography,1012: 151-159.
Bradford, “A Rapid and Sensitive Method for the Quantitation of Microgram Quantities of Protein Utilizing the Principle of Protein-Dye Binding”, (1976),Anal. Biochem.72: 248-254.
Sweeney, “Generic Combustion Method for Determination of Crude Protein in Feeds: Collaborative Study”, (1989),JAOAC,72: 770-774.
Choi et al., “Pressurized liquid extraction of active ingredients (ginsenosides) from medicinal plants using non-ionic surfactant solutions”, (2003),J. Chromatog. A. 983,153-162.
Dubois et al., “Colorimetric Method for Determination of Sugars and Related Substances”, (1956),Anal. Chem.,28: 350-356.
Fox et al., “Miniaturization of Three Carbohydrate Analyses Using a Microsample Plate Reader”, (1990),Anal. Biochem.,195: 93-96.
Oleszek, “Solid-Phase Extraction-Fractionation of Alfalfa Saponins”, (1988), J. Sci. Food Agric., 44: 43-49.
Mazza et al., “Compositional and Morphological Characteristics of Cow Cockle (Saponaria vaccaria) Seed, a Potential Alternative Crop”, (1992),J. Agric. Food Chem.,40: 1520-1523.
Cacace Juan Eduardo
Mazza Giuseppe
Gowling Lafleur Henderson LLP
Heggestad Helen F
Her Majesty the Queen in Right in Canada as Represented by the M
LandOfFree
Extraction of phytochemicals does not yet have a rating. At this time, there are no reviews or comments for this patent.
If you have personal experience with Extraction of phytochemicals, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Extraction of phytochemicals will most certainly appreciate the feedback.
Profile ID: LFUS-PAI-O-2696963