Electrode preconditioning method for a plating bath monitoring p

Chemistry: electrical and wave energy – Processes and products – Processes of treating materials by wave energy

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204402, 204412, 204434, G01N 2726

Patent

active

053244001

ABSTRACT:
A method of preconditioning an electrode for use in a plating bath monitoring process. The method involves applying at least one anodic signal to an electrode in contact with the plating bath solution in order to yield a reproducibly clean and stabilized electrode surface, and then applying a plating signal to deposit a layer of metal on the anodically treated electrode. The resultant preconditioned electrode improves the accuracy and precision of subsequent voltammetric monitoring measurements for a variety of different plating baths. The method is easily integrated with and thereby enhances the capabilities of known voltammetric plating bath monitoring processes.

REFERENCES:
Tench et al., Cyclic Pulse Voltammetric Stripping Analysis of Acid Copper Plating Baths, Jun. 1984, pp. 831-834.

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