Chemistry: molecular biology and microbiology – Micro-organism – tissue cell culture or enzyme using process... – Preparing compound containing saccharide radical
Reexamination Certificate
2005-06-15
2008-08-19
Wilson, James (Department: 1624)
Chemistry: molecular biology and microbiology
Micro-organism, tissue cell culture or enzyme using process...
Preparing compound containing saccharide radical
C435S171000, C435S911000, C435S917000, C435S921000, C536S020000
Reexamination Certificate
active
07413881
ABSTRACT:
A highly deacetylated chitosan obtained from microbial biomass, a method of obtaining chitosan from microbial biomass, and biomass for making chitosan are disclosed. The method includes providing chitin-containing biomass; reacting the chitin-containing biomass in a caustic solution of greater than 25 percent alkali at a reaction temperature greater than 95° C. for a reaction period of at least 10 hours to convert the chitin in the biomass to chitosan; and separating the chitosan from the caustic solution.
REFERENCES:
patent: 2040879 (1936-05-01), Rigby
patent: 3232836 (1966-02-01), Carlozzi et al.
patent: 3632754 (1972-01-01), Balassa
patent: 3903268 (1975-09-01), Balassa
patent: 3911116 (1975-10-01), Balassa
patent: 3914413 (1975-10-01), Balassa
patent: 4056432 (1977-11-01), Slagel et al.
patent: 4282351 (1981-08-01), Muzzarelli
patent: 4806474 (1989-02-01), Hershberger
patent: 4886541 (1989-12-01), Hadwiger
patent: 4948881 (1990-08-01), Naggi et al.
patent: 4970150 (1990-11-01), Yaku et al.
patent: 5219749 (1993-06-01), Bouriotis et al.
patent: 5232842 (1993-08-01), Park et al.
patent: 5262310 (1993-11-01), Karube et al.
patent: 5730876 (1998-03-01), You et al.
patent: 5905035 (1999-05-01), Okada et al.
patent: 5985644 (1999-11-01), Roseman et al.
patent: 5998173 (1999-12-01), Haynes et al.
patent: 6117851 (2000-09-01), Sherman et al.
patent: 6333399 (2001-12-01), Teslenko et al.
patent: 2005/0215774 (2005-09-01), Trinkle et al.
patent: 0 885 954 (1998-12-01), None
patent: 0885954 (1998-12-01), None
patent: 458839 (1936-12-01), None
patent: 55 012109 (1980-01-01), None
patent: 55012109 (1980-01-01), None
patent: 62070401 (1987-03-01), None
patent: 63097633 (1988-04-01), None
patent: 63225602 (1988-09-01), None
patent: 2149335 (1990-06-01), None
patent: 2180903 (1990-07-01), None
patent: 2200196 (1990-08-01), None
patent: 2229832 (1990-09-01), None
patent: 2258740 (1990-10-01), None
patent: 5068580 (1993-03-01), None
patent: 5068580 (1993-10-01), None
patent: 7330808 (1995-12-01), None
patent: 08 041106 (1996-06-01), None
patent: 08041106 (1996-06-01), None
patent: 10297913 (1998-11-01), None
patent: WO 98/42755 (1998-10-01), None
patent: WO 00/04182 (2000-01-01), None
Aiba, S., “Preparation of N-acetylchitooligosaccharides from lysozymic hydrolysates of partially N-acetylated chitosans”Carbohydrate Research, vol. 261, pp. 297-306 (1994).
Alonso, I., et al., “Determination of the Degree of Acetylation of Chitin and Chitosan by Thermal Analysis,”Journal of Thermal Analysis, vol. 28, pp. 189-193 (1983).
Arcidiacono, S. et al., “Molecular Weight Distribution of Chitosan Isolated fromMucor rouxiiunder Different Culture and Processing Conditions,”Biotechnology and Bioengineering, vol. 39, pp. 281-286 (1992).
Bartnicki-Garcia S., “Cell Wall Chemistry, Morphogenesis, and Taxonomy of Fungi,”Chemistry of Fungal Cell Wall, pp. 87-108 (1968).
Benjakul, S. et al., “Improvement of Deacetylation of Chitin from Black Tiger Shrimp (Penaeus monodon) Carapace and Shell,”ASEAN Food Journal, vol. 9, No. 4, pp. 136-140 (1994).
Beri, R. et al., Characterization of Chitosans via Coupled Size-Exclusion Chromatography and Multiple-Angle Laser Light-Scattering Technique,Carbohydrate Research, vol. 238, pp. 11-26 (1993).
Biermann, C., “Hydrolosis and Other Cleavage of Glycosidic Linkages,” Chapter 3, pp. 2941, date unknown.
Carlson, T. et al., “Chitin/Chitosan Extraction fromA. nigerMycelium,”Cargill Central Research, 16 pages (Aug. 1997).
“Chitin/Chitosan Specifications,”Biopolymer Engineering, Inc., http://www.biopolymer.com/spec.htm, 1 page (date printed Mar. 4, 1999).
Davies, D., et al., “Determination of the Degree of Acetylation of Chitin and Chitosan,”Methods in Enzymology, vol. 161, Part B, pp. 442-446 (1988).
Domszy, J. et al., “Evaluation of Infrared Spectroscopic Techniques for Analysing Chitosan,”Makromal. Chem., vol. 186, pp. 1671-1677 (1985).
Farkas, V., et al., “Fungal Cell Walls: Their Structure, Biosynthesis and Biotechnological Aspects,”Acta Biotechnol., vol. 10, No. 3, pp. 225-238 (1990).
Fleet, G., et al., “17 Fungal Glucans—Structure and Metabolism,”Encyclopedia of Plant Physiology, vol. 13B, New Series, pp. 416-440 (1981).
Gassner, G., et al., “Teichuronic Acid Reducing TerminalN-Acetylglucosamine Residue Linked by Phosphodiester to Peptidoglycan ofMicrococcus luteus,”J. Bacteriol., vol. 172, No. 5, pp. 2273-2279 (May 1990).
Gobin, P., et al., “Structural Chemistry of Fungal, Polysaccharides,” pp. 367-417 (1968).
Johnston, I., “The Composition of the Cell Wall ofAsperigillus niger”, Biochem J, vol. 96, pp. 651-658 (1965).
Kurita, K., “Controlled Functionalization of the Polysaccharide Chitin,”Prog. Polym. Sci., vol. 26, pp. 1921-1971 (2001).
Kurita, K., et al., Studies of Chitin, 3, Preparation of Pure Chitin, Poly (N-acetyl-D-glucosamine), from the Water-Soluble Chitin,Makromal. Chem., vol. 178, pp. 2595-2602 (1977).
Kurita, K, et al., “Studies on Chitin, 4, Evidence for Formation of Block and Random Copolymers ofN-Acetyle-D-glucosamine and D-Glucosamine by Hetero- and Homogeneous Hydrolyses,”Makromol. Chem., vol. 178, pp. 3197-3202 (1977).
Mima, S., et al., “Highly Deacetylated Chitosan and Its Properties,”Journal of Applied Polymer Sciences, vol. 28, pp. 1909-1917 (1983).
Maghami, G., et al., “Evaluation of the Viscometric Constants for Chitosan,”Makromol. Chem., vol. 189, pp. 195-200 (1988).
Muzzarelli, R., et al., Chelating, Film-Forming, and Coagulating Ability of the Chitosan-Glucan Complex fromAspergillus nigerIndustrial Wastes,Biotechnology and Bioengineering, vol. 22, pp. 885-896 (1980).
Nanjo, F., et al., “Enzymatic Method for Determination of the Degree of Deacetylation of Chitosan,”Analytical Biochemistry, vol. 193, pp. 164-167 (1991).
Niola F., et al., “A Rapid Method for the Determination of the Degree ofN-acetylation of chitin-chitosan samples by acid hydrolysis and HPLC,”Carbohydrate Research, vol. 238, p. 1-9 (1993).
No, H., et al., “Preparation and Characterization of Chitin and Chitosan—A Review,”Journal of Aquatic Food Product Technology, vol. 4, No. 2, pp. 27-52 (1995).
Novikov, V., et al., “Synthesis of D(+)-Glucosamine Hydrochloride,”Russian Journal of Applied Chemistry, vol. 70, No. 9, pp. 1467-1470 (1997).
Ottoy, M., et al. “Preparative and Analytical Size-exclusion Chromatography of Chitosans,”Carbohydrate Polymers, vol. 31, pp. 253-261 (1996).
Pelletier, A., et al., “Chitin/Chitosan Transformation by Thermo-Mechano-Chemical Treatment Including Characterization by Enzymatic Depolymerization,”Biotechnology and Bioengineering, vol. 36, pp. 310-315 (1990).
Rege, P., et al., “Chitosan Processing: Influence of Process Parameters During Acidic and Alkaline Hydrolysis and Effect of the Processing Sequence on the Resultant Chitosan's Properties,”Carbohydrate Research, vol. 321, Nos. 3-4, pp. 235-245 (Oct. 15, 1999).
Roberts, G., et al., “Determination of the Viscomtric Constants for Chitosan,”Int. J. Biol, vol. 4, pp. 374-377 (Oct. 1982).
Rokem J., et al., “Degradation of Fungal Cell Walls Taking into Consideration the Polysaccharide Composition,”Enzyme Microb. Technol., vol. 8, No. 10, pp. 588-592 (Oct. 1986) (Abstract).
Ruiz-Herrera J., “Chemical Components of the Cell Wall ofAspergillusSpecies,”Archives of Biochemistry and Biophysics, vol. 122, pp. 118-125 (1967).
Sabnis, S., et al., “Improved Infrared Spectroscopic Method for the Analysis ofN-deacetylation of Chitosan,”Polymer Bulletin, vol. 39, pp. 67-71 (1997).
Sannan, T., et al., “Studies on Chitin, 2, Effect of Deacetylation on Solubility,”Makromol. Chem., vol. 177, pp. 3589-3600 (1976).
Shahidi, F., et al., “Food Applications of Chitin and Chitosans,
Bohlmann John A.
Fan Weiyu
Henning Joseph P.
Hwang Ki-Oh
Steinke James Donald
Cargill Incorporated
Klarquist & Sparkman, LLP
Sackey Ebenezer
Wilson James
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