Aromatic hydroxythiol synthesis using diazonium salts

Organic compounds -- part of the class 532-570 series – Organic compounds – Sulfur containing

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568 61, 548544, 549 62, 549476, 549505, C07C31902

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060546220

ABSTRACT:
A method for the preparation of aromatic hydroxythiols including oxidizing an aromatic aminothiol to form an aminodisulfide compound; forming a bis-diazonium salt of the aminodisulfide compound; and reacting the bis-diazonium salt with water to form an aromatic hydroxyldisulfide compound, which is then reduced to the hydroxythiol. New bis-diazonium aromatic disulfide compounds are also disclosed.

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