Apparatus for rapidly drying a wet, porous gel monolith

Drying and gas or vapor contact with solids – Apparatus – Vacuum

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34407, F26B 1330

Patent

active

053436334

ABSTRACT:
A process and apparatus are described for rapidly drying a wet, porous gel monolith of glass or ceramic, at subcritical temperatures without inducing any cracking of the gel. The wet gel is immersed in a liquid solvent in a chamber, and the liquid solvent is then heated and expelled from the chamber. Further heating, with or without the presence of a flowing inert gas, fully dries the wet gel. When an inert gas is used, the gas is delivered to the chamber with a controlled solvent partial vapor pressure, to correspondingly control the driving force for drying the gel.

REFERENCES:
patent: 3270434 (1966-09-01), Hackenburg et al.
patent: 5090132 (1992-02-01), Kobayashi et al.

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