Source alternating MOCVD processes to deposit tungsten...

Semiconductor device manufacturing: process – Coating with electrically or thermally conductive material – To form ohmic contact to semiconductive material

Reexamination Certificate

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C438S627000, C438S643000, C438S653000, C438S679000, C438S680000, C438S681000, C257SE21170, C257SE21584

Reexamination Certificate

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10326712

ABSTRACT:
An alternating source MOCVD process is provided for depositing tungsten nitride thin films for use as barrier layers for copper interconnects. Alternating the tungsten precursor produces fine crystal grain films, or possibly amorphous films. The nitrogen source may also be alternated to form WN/W alternating layer films, as tungsten is deposited during periods where the nitrogen source is removed.

REFERENCES:
patent: 6534395 (2003-03-01), Werkhoven et al.
patent: 2002/0009544 (2002-01-01), McFeely et al.
patent: 2003/0143328 (2003-07-01), Chen et al.
patent: 2003/0198587 (2003-10-01), Kaloyeros et al.
Article entitled, “Low temperature metal-organic chemical vapor deposition of tungsten nitride as diffusion barrier for copper metalization.” by Jean K. Kelsey et al., published in J. Vac. Sci. Technol. B 17(3) May/Jun. 1999, pp. 1101-1104.
Article entitled, “WNxdiffusion barriers between Si and Cu” by Masaki Uekubo et al., published in Thin Solid Films 286 (1996), pp. 170-175.
Article entitled, “Properties of reactively sputtered WNxas Cu diffusion barrier.” by Bong-Seok Suh et al., published in Thin Solid Films 348 (1999), pp. 299-303.

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