Porous protective solid phase micro-extractor sheath

Measuring and testing – Sampler – sample handling – etc. – With constituent separation

Reexamination Certificate

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Details

C073S064560, C073S864010, C073S864710, C422S069000, C422S088000, C422S105000

Reexamination Certificate

active

06871556

ABSTRACT:
A porous protective sheath for active extraction media used in solid phase microextraction (SPME). The sheath permits exposure of the media to the environment without the necessity of extending a fragile coated fiber from a protective tube or needle. Subsequently, the sheath can pierce and seal with GC-MS septums, allowing direct injection of samples into inlet ports of analytical equipment. Use of the porous protective sheath, within which the active extraction media is contained, mitigates the problems of: 1) fiber breakage while the fiber is extended during sampling, 2) active media coating loss caused by physical contact of the bare fiber with the sampling environment; and 3) coating slough-off during fiber extension and retraction operations caused by rubbing action between the fiber and protective needle or tube.

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Zhang et al., “Direct Solid Phase Microextraction of Complex Aqueous Samples With Hollow Fibre Membrane Protection”, Jul. 1996, Royal Society of Chemistry, Analytical Communications vol. 33, No. 7, pp 219-221.

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