Spin-trap molecules 2-trifluoromethyl- of 5,5-dimethyl-1-dyrroli

Details Spin-trap molecules 2-trifluoromethyl- of 5,5-dimethyl-1-dyrroli Spin-trap molecules 2-trifluoromethyl- of 5,5-dimethyl-1-dyrroli

1993-10-22

1995-04-11

Springer, David B.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

C07D20746

Patent

active

054059674

ABSTRACT:
Novel spin traps comprising 2-trifluoromethyl-1-DMPO or derivatives thereof have now been found. An effective synthesis method for these spin traps is also disclosed.

REFERENCES:
Tordeux, et al., "Synthese de la trifluoromethyl-vinyl-cetone," J Fluorine Chemistry 20:301-306 (1982).
Dess, et al., "Readily accessible 12-I-5 oxidant for the conversion of primary and secondary alcohols to aldehydes and ketones," J Org Chem 48:4155-4156 (1983).
Linderman, et al., "Oxidation of fluoroalkyl-substituted carbinols by the Dess-Martin reagent," J Org Chem 54:661-668 (1989).

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