Method for delignification of ligno-cellulose containing fiber m

Paper making and fiber liberation – Processes of chemical liberation – recovery or purification... – With regeneration – reclamation – reuse – recycling or...

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162 40, 162 57, 162 65, 162 89, D21C 912, D21C 914, D21C 1104

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044513321

ABSTRACT:
A method is disclosed for delignification of ligno-cellulose containing fiber material comprising mixing an oxygen-containing gas with the cellulose fiber material so as to atomize the gas and form a foam of the gas and the cellulose fiber material, and without an intervening oxidation step, subjecting the foam to upwardly flowing, substantially non-pressurized, alkali extraction. The alkali extraction step is conducted at a temperature of from about 40.degree. to about 80.degree. C. and at a pH, ligno cellulose containing fiber concentration and oxygen containing gas concentration sufficient to provide a bleached, delignified cellulose fiber without bleaching the lignin substance extracted from the material and to suppress lignin condensation reaction during the extraction.

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patent: 3832276 (1974-08-01), Roymoulik et al.
patent: 3963561 (1976-06-01), Richter
patent: 4053352 (1977-10-01), Hultman
patent: 4104114 (1978-08-01), Rowlandson et al.
patent: 4198266 (1980-04-01), Kirk et al.
"First Oxygen Pulping/Bleaching Seminar Draws High Attendance, Good Papers", Paper Trade Journal, Feb. 28, 1979, pp. 20-24.
"Atmospheric-Pressure Oxygen Bleaching", Eachus; TAPPI; vol. 58, No. 9, pp. 151-154.

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